INSTRUMENT CONTROL PARAMETERS: GCMS -------------------------------------- C:\MSDCHEM\1\METHODS\RSOL_020314_95C_15 MIN_SCAN.M Tue Jun 03 21:25:48 2014 Control Information ------- ----------- Sample Inlet : GC Injection Source : Headspace Mass Spectrometer : Enabled Headspace Parameters Agilent 7697A(GCMS) Instrument Info Address: 146.217.224.45 Serial Number: CN12490025 Firmware Revision: A.01.06 Instrument Settings Vial Pressurization Gas: Helium Loop Size (mL): 3 Keyboard Lock: OFF Transfer Line Type: DB-ProSteel Transfer Line Diameter (mm): 0.53 System Configuration Carrier Control: GC Instrument Resource Conservation Vial Standby Flow (mL/min): 20 Temperature Settings: Oven Temperature (°C): 95 Loop Temperature (°C): 135 Transfer Line Temperature (°C): 150 Timing Settings: Vial Equilibration (min): 15.00 Injection Duration (min): 0.50 GC Cycle Time (min): 42.08 Vial and Loop Settings: Vial Size: 20 Vial Shaking: Level 7, 136 shakes/min with acceleration of 530 cm/s² Fill Mode: Default Fill Pressure (psi): 20 Loop Fill Mode: Default Carrier Settings: Carrier Control Mode: GC controls Carrier Advanced Settings: Extraction Mode: Single Extraction Vent After Extraction: ON Post Injection Purge: Default, 100 mL/min for 1 min Acceptable Leak Check: 0.6mL/min Sequence Actions: Vial Missing:: Skip Wrong Vial Size: Abort Leak Detected: Continue System Not Ready: Abort No Sample Prep method has been assigned to this method. GC Oven Temperature Setpoint On (Initial) 40 °C Hold Time 4 min Post Run 40 °C Program #1 Rate 5 °C/min #1 Value 150 °C #1 Hold Time 0 min #2 Rate 50 °C/min #2 Value 230 °C #2 Hold Time 0 min Equilibration Time 0.25 min Max Temperature 245 °C Slow Fan Disabled Cryo Off Front SS Inlet He Mode Split Heater On 170 °C Pressure On 40 psi Total Flow On 21.404 mL/min Septum Purge Flow On 3 mL/min Gas Saver On 20 After 3 min mL/min Split Ratio 14 :1 Split Flow 17.177 mL/min Thermal Aux 2 (MSD Transfer Line) Temperature Setpoint On (Initial) 230 °C Hold Time 0 min Post Run 0 °C Column Column #1 Flow Setpoint Off (Initial) 1.2269 mL/min Hold Time 0 min Post Run 0.9 mL/min Restek 49915 Rtx-VMS proprietary Crossbond -60 °C—245 °C (245 °C): 40 m x 180 µm x 1 µm In Front SS Inlet He Out MSD (Initial) 40 °C Pressure 40 psi Flow 1.2269 mL/min Average Velocity 34.785 cm/sec Holdup Time 1.9165 min Valve 1 Name ? Type Gas Sampling Valve GSV Loop Volume 1 µL Load Time 0.5 min Inject Time 0.5 min Signals Signal #1: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Front Sample Signal #2: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Front Sample Signal #3: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Front Sample Signal #4: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Front Sample MS ACQUISITION PARAMETERS General Information ------- ----------- Tune File : atune.u Acquistion Mode : Scan MS Information -- ----------- Solvent Delay : 2.80 min EMV Mode : Relative Relative Voltage : 0 Resulting EM Voltage : 1212 [Scan Parameters] Low Mass : 31.0 High Mass : 200.0 Threshold : 150 Sample # : 2 A/D Samples 4 Plot 2 low mass : 50.0 Plot 2 high mass : 550.0 Start Time : 7.80 Low Mass : 42.0 High Mass : 200.0 Threshold : 150 Sample # : 2 A/D Samples 4 Plot 2 low mass : 50.0 Plot 2 high mass : 550.0 [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US12517801 ----------------------------- Trace Ion Detection is OFF. EMISSION : 34.610 ENERGY : 69.922 REPELLER : 30.625 IONFOCUS : 90.157 ENTRANCE_LE : 25.500 EMVOLTS : 1211.765 Actual EMV : 1211.77 GAIN FACTOR : 0.38 AMUGAIN : 1596.000 AMUOFFSET : 119.500 FILAMENT : 1.000 DCPOLARITY : 1.000 ENTLENSOFFS : 18.824 MASSGAIN : -859.000 MASSOFFSET : -38.000 END OF TUNE PARAMETERS ------------------------------------ END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------